D.Gray-Man Filler - All Filler Episodes Lists D.Gray-Man

2021.12.09 08:01 johnrock001 D.Gray-Man Filler - All Filler Episodes Lists D.Gray-Man

D.Gray-Man Filler - All Filler Episodes Lists D.Gray-Man - https://www.myanimeforlife.com/d-gray-man-fille
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2021.12.09 08:01 CKsTechnologyNews proton-gog-install: A mostly automated Windows GOG games install script for Linux/Proton

proton-gog-install: A mostly automated Windows GOG games install script for Linux/Proton submitted by CKsTechnologyNews to CKsTechNews [link] [comments]


2021.12.09 08:01 chairbornebg Обвинения на опозицията към вътрешния министър са довели до боя в турския парламент вчера

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2021.12.09 08:01 trashbag3058 Problems with Fischer indole synthesis

I have been trying to synthesize a certain monoindole on a bridged, C2-symmetrical tricyclic diketone scaffold. So far, I haven't been able to isolate my target product. I have tried different temps (50-70C), tried carrying out the reactions in MeOH and EtOH (both extra dry and pure), tried different acids (methanolic HCl, aq. HCl, AcOH). The phenylhydrazine is pure, I have checked the NMR spectrum. I should probably mention that this compound also includes a tertiary amine.
I can see the product spot on my TLCs (someone who has worked before in this project has synthesised this compound successfully, so I have a standart I can compare my TLC with. Unfortunately they quit their job 5 years ago and now I was told to continue the job). But when it comes to purification, for some reason three spots with Rf values of 0.5, 0.4 and 0.25 (CHCl3:MeOH 10:1) leave the column at once and dilute to 5-8 fractions. I have tried different eluents (CHCl3:MeOH 40:1, 30:1, 20:1, EA:iPrOH 9:1, 5:1 + 1% TEA, I even tried pure MeOH once out of total desperation), but so far no success. Once I managed to get down to 2 spots, unfortunately they do not separate even though I see Rf difference when I elute with MeOH.
If you have any clue how to help me - please share. I am slowly losing my mind and the deadlines are creeping up on me. My supervisor has no idea what to do (frankly I don't think he cares that much). There is no literature on this specific reaction, because it 's a part of a new total synthesis. Thank you in advance.
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2021.12.09 08:01 chairbornebg Китай одобри лекарство срещу КОВИД-19

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2021.12.09 08:01 chay2508 Scary alien game

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2021.12.09 08:01 johnrock001 Rurouni Kenshin Filler - Complete Episode and Filler List

Rurouni Kenshin Filler - Complete Episode and Filler List - https://www.myanimeforlife.com/rurouni-kenshin-fille
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2021.12.09 08:01 ToxicThing Vienna Stadtpark

Vienna Stadtpark submitted by ToxicThing to pics [link] [comments]


2021.12.09 08:01 evanthebouncy My bullied crayfish waited until the big one failed a molt then chewed its face off

My bullied crayfish waited until the big one failed a molt then chewed its face off submitted by evanthebouncy to natureismetal [link] [comments]


2021.12.09 08:01 The_Lobster6 I’ve seen no mention of the leather jacket in all the recent posts, price lists & co (article from WWD)

I’ve seen no mention of the leather jacket in all the recent posts, price lists & co (article from WWD) submitted by The_Lobster6 to Golfwang [link] [comments]


2021.12.09 08:01 botnlausnt Vent Finance and Lossless have teamed up to provide a safe solution for token minting and hack mitigation in the blockchain space. Token issuance on VentUp will be simplified and made more secure with Lossless.

Vent Finance and Lossless have teamed up to provide a safe solution for token minting and hack mitigation in the blockchain space. Token issuance on VentUp will be simplified and made more secure with Lossless. submitted by botnlausnt to AltcoinAdvisor [link] [comments]


2021.12.09 08:01 agnclay IOC evacuates 300 athletes from Afghanistan and pledges $560,000 in ‘humanitarian aid’ for those left behind

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2021.12.09 08:01 Select_Lie1973 33/M Indian, graduated from The University of Texas at Arlington, MS in Computer Science, 3.5 GPA

I have 6 years of IT experience now. I graduated in 2017 but due to my father's declining health, I had to come back to India in an emergency without being able to apply or join a job in the US. Currently in india working for a well known fintech company. I really want to go back to the US and work there. All the hard work I put in for my graduation seems wasted. Used up all my saving for my graduation and now I don't even earn enough here. People don't seem to find my knowledge or my expertise worthy of a decent salary even after getting exceptional performer(yearly rating) twice in 3 years, I don't get to earn enough. I do not have work visa for the US since I had to leave the US in an emergency when I was on OPT period. And didn't had the job offer when I left the US in that rush. I feel lost, tired and disheartened of my never ending struggle. I do not give up because I want my parents to feel proud of me. I want to give them all the comfort I can but at times feel helpless. My fear of getting unemployed keeps me from moving forward or take a jump to another job or resign from the current one(where I am mistreated and underpaid). I am the only bread earner in the house. it seems I have lost all the confidence in myself. I feel I have made all the wrong choices in life. I don't know what I am doing and where I am heading.
submitted by Select_Lie1973 to findapath [link] [comments]


2021.12.09 08:01 Gecko_alt I always get anxious about v* when I’m on my period

I’ve never TU from my period pain, but I know people who have (none family, just friends). I always get worried on my period because I worry I will get s*, though in the years of worrying, I never have. Anyone else have a similar problem?
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2021.12.09 08:01 CronoDroid EVERGLOW - Episode 1 @ EVERGLOW's PICK (211209)

EVERGLOW - Episode 1 @ EVERGLOW's PICK (211209) submitted by CronoDroid to kpop [link] [comments]


2021.12.09 08:01 Ionceburntpasta Amp/DAC for HD 560S

A few weeks ago, I bought a HD 560S which I absolutely admire. I run them from my laptop mostly. I'm looking to know if Amp/DAC is necessary and what would be a budget option at 100€.
Thanks
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2021.12.09 08:01 johnrock001 Yu Yu Hakusho Filler - Filler Guide for Yu Yu Hakusho

Yu Yu Hakusho Filler - Filler Guide for Yu Yu Hakusho - https://www.myanimeforlife.com/yu-yu-hakusho-fille
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2021.12.09 08:01 TarodevOfficial Extend base unity classes using extension methods. Vital beginner programming knowledge

Extend base unity classes using extension methods. Vital beginner programming knowledge submitted by TarodevOfficial to Unity3D [link] [comments]


2021.12.09 08:01 MiniozJoe A little thing i made to celibrate "sam & max beyond time and space" remaster

A little thing i made to celibrate submitted by MiniozJoe to SamandMax [link] [comments]


2021.12.09 08:01 Sussy_Neet Balls

Balls submitted by Sussy_Neet to OkBuddyAzurLane [link] [comments]


2021.12.09 08:01 santi2021 found this little friend in my backyard while watering the plants, how do I clean/wash it?

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2021.12.09 08:01 SamDekkerBot Official: [Roster Moves] - December 09 2021

IF YOU CANNOT SEE COMMENTS, CHANGE THE SORT METHOD OF THE COMMENTS TO SOMETHING DIFFERFENT AND THEN CHANGE IT BACK TO HOW YOU LIKE IT. Post all waiver wire questions here. Separate posts will be deleted. You can also join our Discord server to ask for help there. Click here to find out more about how to create a poll in your comment.
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2021.12.09 08:01 weliveinasamaj Toilet witch wont let me poo in toilet

Toilet witch wont let me poo in toilet submitted by weliveinasamaj to Samaj [link] [comments]


2021.12.09 08:01 maerwald X1 Extreme distorted display (busted?)

https://imgur.com/a/nl6xicz
I'm usually running external monitors and have the integrated display turned off. Now I started travelling and this happened after booting into Fedora 34.
The laptop is only a year old. I'm pretty shocked that this happens with hardware that I paid almost 3k € for.
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2021.12.09 08:01 Opening_Safe5990 Will the Mos be possible

If there will be inventors who will make Mos possible in real life
View Poll
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